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The composition profile of dense part of the oxide scale (≤2 mkm ) on the surface of Zircaloy-4 (SRA) taken across the metal/oxide interface after 90-day testing in liquid water heated up to 360 °C ; the dotted vertical lines separate “black zircon”, ZrO, from zirconium and dense hypo-stoichiometric zirconia, ZrO2−x.
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