Open Access
Table 2
Oxidation results.
| Sample | Time | Initial hydrogen content | Final hydrogen content | ZrO2 layer thickness | α(O) layer thickness | Measured ECR | ECR-CP | α(O) phase fraction |
|---|---|---|---|---|---|---|---|---|
| (#) | s | wppm | wppm | μm | μm | % | % | % |
| AR-1 | 624 | 11 ± 5 | 18 ± 2 | 71 | 92 | 23.6 | 25 | 66 |
| AR-2 | 400 | 11 ± 5 | 15 ± 2 | 58 | 79 | 19.6 | 20 | – |
| AR-3 | 196 | 11 ± 5 | 15 ± 2 | 44 | 59 | 14.7 | 14 | – |
| H64-3 | 624 | 144 ± 17 | 214 ± 19 | 74 | 96 | 24.2 | 25 | 76 |
| H64-5 | 400 | 147 ± 17 | 210 ± 20 | 59 | 81 | 20.2 | 20 | 58 |
| H64-7 | 196 | 173 ± 24 | 219 ± 26 | 44 | 59 | 14.9 | 14 | 32 |
| H60-3 | 624 | 305 ± 39 | 396 ± 35 | 72 | 100 | 23.8 | 25 | 62 |
| H60-5 | 400 | 287 ± 32 | 376 ± 34 | 58 | 80 | 19.0 | 20 | 51 |
| H60-7 | 196 | 305 ± 38 | 356 ± 34 | 42 | 59 | 14.1 | 14 | 27 |
| H66-3 | 624 | 92 ± 12 | 116 ± 10 | 74 | 104 | 23.9 | 25 | 79 |
| H66-5 | 400 | 86 ± 9 | 114 ± 11 | 57 | 82 | 19.8 | 20 | 61 |
| H66-7 | 196 | 92 ± 12 | 104 ± 11 | 43 | 58 | 14.3 | 14 | 45 |
| H58-3 | 624 | 149 ± 17 | 199 ± 17 | 68 | 92 | 23.8 | 25 | 67 |
| H58-5 | 400 | 157 ± 18 | 202 ± 18 | 58 | 78 | 19.7 | 20 | 51 |
| H58-7 | 196 | 165 ± 18 | 191 ± 18 | 43 | 59 | 15.1 | 14 | 30 |
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