Open Access
Table 2
Low temperature oxidation conditions and 900 °C oxidation results for the test matrix.
| 470 °C wet-air oxidation | 900 °C steam oxydation | |||||||
|---|---|---|---|---|---|---|---|---|
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| Test Matrix | Sample | Time | ZrO2 layer thickness ±1 μm |
Time | ZrO2 layer thickness ±1 μm |
α(O) layer thickness ±1 μm |
[H] | Measured ECR |
| (#) | (#) | (days) | (μm) | (min) | (μm) | (μm) | (wppm) | (%) |
| 1 | CCT1 | 15 | 8 | 15 | 8 | 28 | 430 ± 50 | 1.2 |
| CCT2 | 15 | 8 | 30 | 10 | 22 | 590 ± 60 | 3.2 | |
| CCT3 | 15 | 8 | 15 | 8 | 28 | 430 ± 40 | 1.2 | |
| CCT4 | 15 | 8 | 30 | 10 | 30 | 610 ± 80 | 3.2 | |
| 2 | CCT5 | 15 | 7.5 | 5 | 7.5 | 19 | 370 ± 50 | 0.0 |
| CCT6 | 15 | 7.5 | 15 | 9.5 | 31 | 630 ± 100 | 1.2 | |
| CCT7 | 15 | 6.5 | 30 | 9.5 | 36 | 700 ± 90 | 3.4 | |
| CCT8 | 20 | 9.5 | 60 | 22 | 26 | 970 ± 110 | 5.5 | |
| CCT9 | 20 | 9.5 | 60 | 22 | 27 | 1060 ± 110 | 5.5 | |
| CCT10 | 20 | 9.5 | 60 | 24.5 | 27 | 1030 ± 100 | 5.5 | |
| 3 | AT1 | 20 | 9.5 | 60 | 22 | 30 | 970 ± 120 | 5.5 |
| AT2 | 20 | 9.5 | 1060 ± 110 | 5.5 | ||||
| AT3 | 20 | 10 | 60 | 27.5 | 26 | 1070 ± 120 | 5.5 | |
| AT4 | 15 | 8 | 5 | 7.5 | 12 | 370 ± 50 | 0.0 | |
| AT5 | 15 | 8 | 15 | 9.5 | 19 | 630 ± 100 | 1.2 | |
| AT6 | 15 | 8 | 30 | 9.5 | 36 | 700 ± 160 | 3.4 | |
| AT7 | 0 | 0 | 15 | 13 | 21 | 40 ± 20 | 3.8 | |
| AT8 | 0 | 0 | 30 | 16.5 | 20 | 40 ± 10 | 4.8 | |
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