Open Access
Table A.1
Acquisition parameters of the experimental EBSD maps.
Parameter | Value |
---|---|
Microscope | |
Accelerating voltage | 30 kV |
Current | 75 nA |
Focus | Set on the EBSD scan generator |
Working distance | 17 mm |
Acquisition step | 250 nm |
Analyzed zone area | 350 × 350 μm2 |
Grid type | Square |
Points | 1 960 000 |
Acquisition speed | 252 fps |
Exposure time | 3918 μs |
EBSD resolution | 160 × 160 pixels |
Indexation (OIM Data Collection 5.32) | |
Phases | Ni |
Binned pattern size | 160 |
Theta step size | 0.5° |
Min - max peak count | 3-7 |
Min peak magnitude | 3 |
Min peak distance | 10 |
Peak symmetry | 89% |
Hough type | Classic |
Hough resolution | Low |
Convolution mask | 9 × 9 |
Treatment (OIM Analysis 6.1.3) | |
Data filter | Removal of CI <0,1 |
Data count interval (for stat representation) | 0.02° |
KAM representation | 1st neighbours |
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